Journal
GREEN CHEMISTRY
Volume 22, Issue 16, Pages 5262-5266Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0gc01360a
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Funding
- CAPES
- CNPq [401541/2016-9]
- FACEPE [APQ-0549-1.06/17/INCT]
- [309778/2018-2]
- [PQ2-306132/2017-6]
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The electrochemical generation of sulfinyl radicals from commercially available and non-expensive sodium salts of sulfinic acids is described. Electrooxidation reactions were carried out in a graphite powder macroelectrode using an aqueous electrolyte and cavity cell. Further reaction with primary or secondary amines gave the corresponding sulfonamides, a unit present in several biologically active compounds and pharmaceuticals, in good yields.
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