Journal
INORGANIC CHEMISTRY
Volume 56, Issue 7, Pages 4065-4071Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.inorgchem.7b00025
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Funding
- National Natural Science Foundation of China [21274165]
- Distingulished Profssor Research Fund from Central South University of China
- Ministry of Science and Technology of Taiwan [MOST105-2119M-002-029]
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Three approaches have been carefully examined in order to develop a terpyridine-based dendritic metallotriangle; (1) direct self assembly of two types of organic polyterpyridines with metal ions; (2) assembly of flexible metallo-organic ligands containing two uncomplexed free terpyridines with a possible 60 degrees-V-shaped orientation; (3) assembly of functionalized metallotriangles possessing a fixed 60 degrees-bent uncoordinated bisterpyridine. Only the third approach has successfully given rise to the desired first-generation dendritic metallotriangle. Structural characterization was accomplished by NMR, ESI-TWIM-MS, and AFM.
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