Journal
HETEROCYCLES
Volume 101, Issue 1, Pages 223-234Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.3987/COM-19-S(F)16
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Funding
- JSPS KAKENHI [JP 15H05485, 18K19078, JP 17H06092]
- Grants-in-Aid for Scientific Research [18K19078] Funding Source: KAKEN
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A Rh(III)-catalyzed C-H acetoxylation of 2-pyridones with phenyliodine(III) diacetate (PIDA) in a DCE/AcOH mixed solvent system has been developed using N-2-pyridyl function as directing group. The reaction occurs under mild conditions, typically in air at 40 degrees C, to selectively produce the corresponding C6-acetoxylated 2-pyridones in moderate to good yields.
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