Journal
JOURNAL OF THE ELECTROCHEMICAL SOCIETY
Volume 167, Issue 15, Pages -Publisher
ELECTROCHEMICAL SOC INC
DOI: 10.1149/1945-7111/abb8f7
Keywords
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Funding
- KSTEPS, DST, GOVT. OF KARNATAKA
- DST-Nanomission, Govt of India [SR/NM/NT-1026/2017]
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A facile electrochemical oxidation of pyridyl carbinol based on Manganese dioxide-Phosphate (MnO2-Pi) was fabricated by electro-deposition of MnO2-Pi on Porous carbon nanospheres (PCN) modified carbon fiber paper (CFP) electrode. A simple working electrode was developed initially by coatingMonkey Pod(MP) derived PCN on carbon fiber paper (CFP) electrode. Voltammetric deposition of MnO2-Pi on PCN/CFP electrode was carried out in an electrolyte containing phosphate buffer and KMnO4. The modified electrodes (PCN/CFP and MnO2-Pi-PCN/CFP) were characterized by different physicochemical methods and electroanalytical techniques like cyclic voltammetry and AC impedance spectroscopy. Inorganic phosphate (Pi) and MnO(2)centers present on PCN/CFP electrode plays a major role towards oxidation of pyridyl carbinol electrochemically. The proposed MnO2-Pi-PCN/CFP electrode was effectively applied for the electrochemical oxidation of pyridyl carbinol in TEMPO medium.
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