Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2020, Issue 40, Pages 6368-6369Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.202001088
Keywords
Amination; Amines; EPR spectroscopy; Pyrrolidines; Radicals
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The initial steps of the catalytic Hofmann-Loffler reaction include the formation of theN-halogenated amine with further formation of a nitrogen-centered radical. We had reported the presence and detection of a radical through EPR spectroscopy. Based on new data, we discuss the observed EPR signal.
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