Journal
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY
Volume 35, Issue 10, Pages 2239-2247Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0ja00144a
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Funding
- JSPS KAKENHI [JP17K14506, JP19K05082, JP20K15314]
- Hyogo Science and Technology Association
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Laser-induced breakdown spectroscopy (LIBS) of dry residues on a solid substrate is a promising method for microanalysis of liquid samples. In this work, a hydrophilized porous silicon (Si) substrate loaded with gold nanoparticles was applied in LIBS of dry residues for signal enhancement. The porous Si substrate was prepared by a simple wet process,i.e.metal-assisted etching. A 5 mu L strontium chloride aqueous solution was dried on the porous Si substrate and the dry residue was analyzed by a single-pulse scheme with a laser energy of 1.5 mJ per pulse. We successfully enhanced the strontium signal intensity over 150 times by using the porous Si substrate instead of a flat Si substrate. We also demonstrated that the signal intensity changed depending on the pore depth of the porous Si. The porous Si has great potential as a substrate for LIBS of dry residues.
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