Journal
NATURE COMMUNICATIONS
Volume 11, Issue 1, Pages -Publisher
NATURE RESEARCH
DOI: 10.1038/s41467-020-19629-5
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Funding
- National Natural Science Foundation of China [51922082, 51971170, 51942104]
- National Key Research and Development Program of China [2017YFB0702301]
- 111 Project of China [BP2018008]
- Innovation Project of Shaanxi Province [2017KTPT-12]
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Zirconium alloys are widely used structural materials of choice in the nuclear industry due to their exceptional radiation and corrosion resistance. However long-time exposure to irradiation eventually results in undesirable shape changes, irradiation growth, that limit the service life of the component. Crystal defects called < c > loops, routinely seen no smaller than 13nm in diameter, are the source of the problem. How they form remains a matter of debate. Here, using transmission electron microscopy, we reveal the existence of a novel defect, nanoscale triangle-shaped vacancy plates. Energy considerations suggest that the collapse of the atomically thick triangle-shaped vacancy platelets can directly produce < c > dislocation loops. This mechanism agrees with experiment and implies a characteristic incubation period for the formation of < c > dislocation loops in zirconium alloys. Zirconium alloys are widely used in the nuclear industry, but long-time irradiation leads to shape changes and irradiation growth that relate to basal dislocation loops in zirconium. Here the authors discern nanoscale triangle-shaped vacancy platelets in helium-irradiated zirconium, which are a precursor of basal dislocation loops.
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