Journal
CHEMICAL COMMUNICATIONS
Volume 56, Issue 95, Pages 15020-15023Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0cc06834a
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Funding
- Northwestern Polytechnical University
- Fundamental Research Funds for the Central Universities [31020200QD046]
- Natural Science Foundation of Jiangsu Province [BK20171463]
- MOE [M4012045.110 RG12/18-(S)]
- Nanjing Tech University
- Nanyang Technological University
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A simple and practical method to access N-substituted 2-pyridones via a formal [3+3] annulation of enaminones with acrylates based on Rh-III-catalyzed C-H functionalization was developed. Control and deuterated experiments led to a plausible mechanism involving C-H bond cross-coupling and aminolysis cyclization. This strategy provides a short synthesis of structural motifs of N-substituted 2-pyridones.
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