4.1 Article

Comprehensive study of crystalline AlN/sapphire templates after high-temperature annealing with various sputtering conditions

Journal

JOURNAL OF SEMICONDUCTORS
Volume 41, Issue 12, Pages -

Publisher

IOP PUBLISHING LTD
DOI: 10.1088/1674-4926/41/12/122802

Keywords

sputter; annealing; AlN; dislocation density

Funding

  1. National Key R&D Program of China [2016YFB0400800, 2017YFB0404202]
  2. National Natural Sciences Foundation of China [61527814, 61674147, 61904176, U1505253]
  3. Beijing Nova Program [Z181100006218007]
  4. Youth Innovation Promotion Association [CAS 2017157]

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High-quality AlN/sapphire templates were fabricated by the combination of sputtering and high-temperature (HT) annealing. The influence of sputtering parameters including nitrogen flux, radio frequency power, and substrate temperature on the crystalline quality and surface morphology of annealed AlN films were investigated. With lower substrate temperature, lower power, and lower N-2 flux, the full width at half maximum of the X-ray rocking curve for AlN (0002) and (10 (1) over bar2) were improved to 97.2 and 259.2 arcsec after high-temperature annealing. This happens because the increased vacancy concentration of sputtered AlN films can facilitate the annihilation of dislocations by increasing the recovery rate during HT annealing. Step and step-bunching morphologies were clearly observed with optimized sputtering conditions.

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