4.5 Article

Xylitol pentanitrate - Its characterization and analysis

Journal

FORENSIC SCIENCE INTERNATIONAL
Volume 316, Issue -, Pages -

Publisher

ELSEVIER IRELAND LTD
DOI: 10.1016/j.forsciint.2020.110472

Keywords

Xylitolpentanitrate; Analysis; Mass spectrometry; Raman; NMR; Infrared; Gas chromatography; Liquid chromatography; Nitrate esters; Explosives

Funding

  1. Microscopy Australia
  2. Australian National Fabrication Facility (ANFF) at the South Australian nodes under the National Collaborative Research Infrastructure Strategy
  3. Defence Science and Technology Group via the Centre of Expertise in Energetic Materials

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Xylitol is a polyhydric alcohol that may be nitrated to form an explosive (xylitol pentanitrate or XPN). Consequently, forensic and first response personnel may encounter XPN in post-blast residues or as a bulk material. Despite this, key analytical data for XPN that may be used in first response or forensic operations to aid its detection are not yet available in the literature. The present article provides infrared spectrometry, Raman spectrometry, nuclear magnetic resonance spectrometry, chromatography and mass spectrometry data in order to address this knowledge gap. (C) 2020 Elsevier B.V. All rights reserved.

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