4.7 Article

Investigation of microstructure and selected properties of Al2O3-Cu and Al2O3-Cu-Mo composites

Journal

ADVANCED COMPOSITES AND HYBRID MATERIALS
Volume 4, Issue 1, Pages 212-222

Publisher

SPRINGERNATURE
DOI: 10.1007/s42114-020-00188-8

Keywords

Composites; Slip casting; Mechanical properties; Scanning electron microscopy

Funding

  1. National Science Centre within the framework of the research project OPUS 13 [2017/25/B/ST8/02036]
  2. Foundation for Polish Science (FNP) - START 2019 scholarship

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The study focused on the fabrication and characterization of Al2O3-Cu and Al2O3-Cu-Mo ceramic-metal composites, with molybdenum addition improving the wear resistance properties of the composites.
The scope of work included the fabrication of ceramic-metal composites from the Al2O3-Cu and Al2O3-Cu-Mo and examining their microstructure and selected properties. The composites were fabricated by the slip casting method. The rheological behavior, microstructures, X-ray analysis, and mechanical properties were investigated. The rheological study demonstrated that all of the obtained slurries were non-Newtonian shear diluted fluids and stability on time. In both slurries, the flow limit is close to 0 Pa, which is very beneficial when casting the suspensions into molds. The X-ray analysis reveals Al2O3, Cu, and Mo phases in all specimens. No new phases were found in both types of composites after the sintering process. The results provided that the hardness for Al2O3-Cu-Mo composites was equal to 10.06 +/- 0.49 GPa, while for Al2O3-Cu, it was equal to 6.81 +/- 2.08 GPa. The K-1C values measured, with the use of Niihara equation, for composites with and without the addition of Mo were equal to 6.13 +/- 0.62 MPa m(0.5) and 6.04 +/- 0.55 MPa m(0.5), respectively. It has been established that the mean specific wear rates of Al2O3-Cu and Al2O3-Cu-Mo samples were 0.35 x 10-5 +/- 0.02 mm(3) N-1 m(-1) and 0.22 x 10-5 +/- 0.04 mm(3) N-1 m(-1), respectively. It was found that molybdenum addition improved wear resistance properties of the composites.

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