4.0 Article

Effects of heating on the physical properties of premixed calcium silicate-based root canal sealers

Journal

JOURNAL OF ORAL SCIENCE
Volume 63, Issue 1, Pages 65-69

Publisher

NIHON UNIV, SCHOOL DENTISTRY
DOI: 10.2334/josnusd.20-0325

Keywords

calcium silicate-based sealers; heat-induced changes; heating; physical properties; warm vertical condensation

Funding

  1. Japan Society for the Promotion of Science (KAKENHI) [17K11700]
  2. Grants-in-Aid for Scientific Research [17K11700] Funding Source: KAKEN

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Heating calcium silicate-based root canal sealers accelerates setting time, decreases flow, and increases film thickness, with varying degrees of impact depending on the product used.
The purpose of this study was to examine the effect of heating on the physical properties of four types of premixed calcium silicate-based root canal sealers. Endoseal MTA, Well-Root ST, EndoSequence BC Sealer, EndoSequence BC Sealer HiFlow, and AH Plus (epoxy resin root canal sealer) were heated at 100 degrees C for 1 min, and changes in setting time, flow, and film thickness were evaluated in accordance with ISO 6876:2012 standards. In addition, pH measurement and scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS) analyses of the set materials were performed. All root canal sealers heated at 100 degrees C showed significant decreases in setting time and flow, particularly Endoseal MTA. In addition, the film thickness of Endoseal MTA increased significantly after heating at 100 degrees C. The pH and SEM/EDS results were not affected by heating. !leafing calcium silicate-based root canal sealers accelerated setting time. decreased flow, and increased film thickness. However, the degree of these changes varied among the products. The present findings indicate that heat-induced changes in the physical properties of calcium silicate-based root canal sealers could adversely affect the quality of warm vertical condensation technique.

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