Journal
CHINESE CHEMICAL LETTERS
Volume 32, Issue 1, Pages 136-139Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/j.cclet.2020.11.059
Keywords
Catalyst-free; Arylazo sulfones; 1,6-Enynes; Sulfonylated gamma-butyrolactams
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Funding
- International Cooperation Project of Qinghai Province [2018-HZ-806]
- Youth Innovation and Technology Project of Higher School in Shandong Province [2019KJC021]
- Natural Science Foundation of Shandong Province [ZR2018MB009]
- Qinghai Key Laboratory of Tibetan Medicine Research [2017-ZJ-Y11]
- CAS Light of West China Program 2018
- Entrepreneurship Training Program for College Students [201910049]
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A convenient and regioselective sulfonylation/cyclization method has been developed for the synthesis of sulfonylated gamma-butyrolactams. The reaction can be efficiently conducted under catalyst- and additive-free conditions, selectively constructing C-S and C-C bonds in one-pot procedure.
A convenient and regioselective sulfonylation/cyclization of 1,6-enynes with arylazo sulfones has been developed to access a series of sulfonylated gamma-butyrolactams. The present reaction could be efficiently conducted under catalyst- and additive-free conditions, in which C-S and C-C bonds were selectively constructed in one-pot procedure. (C) 2020 Chinese Chemical Society and Institute of Materia Medica, Chinese Academy of Medical Sciences. Published by Elsevier B.V. All rights reserved.
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