Journal
CHEMICAL COMMUNICATIONS
Volume 57, Issue 37, Pages 4556-4559Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d1cc00393c
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Funding
- European Regional Development Fund [ERDF Interreg Va programme] [121]
- EPSRC [EP/P013341/1, EP/L003325/1, EP/K039466/1]
- EPSRC [EP/L003325/1, EP/P013341/1, EP/K039466/1] Funding Source: UKRI
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A new route to azocines and benzoazocines from furopyridinones is described through a photochemically induced [1,3]-sigmatropic rearrangement. The method provides excellent atom economy by sequencing thermal and photochemical ring expansion steps under continuous flow.
A new route to azocines and benzoazocines from furopyridinones is described through a photochemically induced [1,3]-sigmatropic rearrangement. The method gives access to these 8-membered nitrogen heterocycles from dimethyl squarate in four stages and with excellent atom economy by sequencing thermal and photochemical ring expansion steps under continuous flow.
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