Journal
CHEMICAL COMMUNICATIONS
Volume 57, Issue 66, Pages 8210-8213Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d1cc03009d
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Funding
- Natural Sciences and Engineering Research Council of Canada [RGPIN-2018_101694]
- Canada Research Chair
- Florida State University
- National High Magnetic Field Laboratory (NHMFL) - National Science Foundation [DMR-1644779]
- State of Florida
- University of Windsor
- Canadian Foundation for Innovation
- Ontario Innovation Trust
- Natural Sciences and Engineering Research Council [RGPIN-2016_06642]
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An H-shaped [2]rotaxane composed of a bis(benzimidazole) axle and a 24-membered crown ether wheel with four trityl groups forms a highly crystalline material allowing large amplitude motion of the interlocked macrocycle, characterized using variable-temperature (VT) H-2 solid-state nuclear magnetic resonance (SSNMR).
An H-shaped [2]rotaxane comprising a bis(benzimidazole) axle and a 24-membered crown ether wheel appended with four trityl groups forms a highly crystalline material with enough free volume to allow large amplitude motion of the interlocked macrocycle. Variable-temperature (VT) H-2 solid-state nuclear magnetic resonance (SSNMR) was used to characterize the dynamics of the [2]rotaxane wheel in this material.
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