Journal
CHEMICAL COMMUNICATIONS
Volume 57, Issue 87, Pages 11513-11516Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d1cc04080d
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- ARC [DP190100798, 13]
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A series of formamidinatoiodidolanthanoid(iii) complexes have been synthesized in good yields by direct reactions of free metals with iodine and DFFormH or DippFormH in appropriate ratios, and are stable without rearrangement.
A number of formamidinatoiodidolanthanoid(iii) complexes, [Ln(DFForm)(2)I(thf)(2)] and [Ln(DFForm)I-2(thf)(3)] (DFFormH = N,N '-bis(2,6-difluorophenyl)formamidine) and [Ln(DippForm)I-2(thf)(3)] (DippFormH = N,N '-bis(2,6-diisopropylphenyl)formamidine) have been synthesized in good yields by one-pot direct reactions of the corresponding free metals with iodine and DFFormH or DippFormH in suitable ratios and are stable to rearrangement.
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