Journal
CHEMICAL COMMUNICATIONS
Volume 57, Issue 87, Pages 11481-11484Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d1cc04813a
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Funding
- National Natural Science Foundation of China [21901041]
- State Key Laboratory of Physical Chemistry of Solid Surfaces, Xiamen University [202008]
- Hundred-Talent Project of Fujian [50012742]
- Fuzhou University [510841]
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An environmentally friendly and efficient electrochemical method has been developed for the synthesis of beta-fluorosulfones from styrenes using sulfonylhydrazides and triethylamine trihydrofluoride. The reaction conditions are mild and have a broad substrate scope, easily scalable to gram-scale preparation.
An environmentally friendly and efficient electrochemical fluorosulfonylation of styrenes has been developed. With the use of sulfonylhydrazides and triethylamine trihydrofluoride, a diverse array of beta-fluorosulfones could be readily obtained. This reaction features mild conditions and a broad substrate scope, which could also be conveniently extended to a gram-scale preparation.
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