Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 19, Issue 44, Pages 9654-9658Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d1ob01960k
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A Mn(III)-promoted thiocarbonylation procedure for the synthesis of thioesters has been developed, using easily available starting materials and cheap and non-toxic promoter Mn(OAc)(3)·2H(2)O, resulting in a broad range of thioesters synthesized in good to excellent yields via radical intermediates.
A Mn(iii)-promoted thiocarbonylation procedure toward the synthesis of thioesters has been developed. By employing easily available disulfides and potassium alkyltrifluoroborates as the starting materials, and cheap and non-toxic Mn(OAc)(3)center dot 2H(2)O as the promotor, a broad range of thioesters were synthesized in good to excellent yields via radical intermediates.
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