Journal
CHEMICAL COMMUNICATIONS
Volume 57, Issue 91, Pages 12167-12170Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d1cc05263b
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Funding
- PMRF
- CSIR
- [INT/RUS/RFBR/359]
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A new protocol has been developed for mono- and bis-ortho-C-H alkynylation of easily accessible benzamide derivatives using alkynyl bromides at room temperature by combining cobalt and photocatalysts. Different alkynyl bromides have shown diverse reactivity towards C-H alkynylation and competing C-H/N-H bond annulation reactions, resulting in good yields with excellent functional group tolerance.
A new protocol is developed for the mono- and bis-ortho-C-H alkynylation of easily accessible benzamide derivatives using alkynyl bromides at room temperature by merging cobalt and photocatalysts. The diverse reactivity of various alkynyl bromides towards the C-H alkynylation and competing C-H/N-H bond annulation reactions has been demonstrated to give the corresponding products in good yields with excellent functional group tolerance.
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