Journal
TRANSACTIONS OF NONFERROUS METALS SOCIETY OF CHINA
Volume 31, Issue 9, Pages 2615-2625Publisher
ELSEVIER
DOI: 10.1016/S1003-6326(21)65680-7
Keywords
Mg-Nd-Zn-Zr alloy; drawing; annealing; mechanical properties; corrosion rate
Categories
Funding
- National Natural Science Foundation of China [U1804251]
- Shanghai Municipal Commission of Economy and Information, China [GYQJ-2019-1-27]
- Science and Technology Commission of Shanghai Municipality, China [18441908000, 19441906300, 19441913400]
- Shenzhen's Three Renowned Project, China [SZSM201612092]
- Shanghai Jiao Tong University Medical-engineering Cross Fund, China [YG2019ZDA02]
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Research shows that annealing at slightly elevated temperature for short time can improve the properties of JDBM wires, such as finer grain size and more dispersive distribution of precipitates. Annealing at 350 degrees C for 5 minutes is identified as the optimal parameters for further fabrication of fine wires.
Mg-Nd-Zn-Zr magnesium alloy (JDBM) has been studied widely as biodegradable medical material. To process high quality JDBM wires, effects of annealing on the mechanical properties and degradation behavior after drawing were studied by microscopic observations, tensile and immersion tests. The as-extruded wires with a diameter of 3 mm could be drawn up to 9 passes without annealing until 125% cumulative drawing deformation. Complete recrystallization occurred after annealing at 325 degrees C for 30 min, 350 degrees C for 5 min or 450 degrees C for 3 min, respectively. Room temperature tensile tests and simulated body fluid immersion tests showed that annealing at slightly elevated temperature for short time could obtain better properties due to the finer grain size and more dispersive distribution of precipitates. For this study, annealing at 350 degrees C for 5 min is the best parameters which can be utilized to further fabricate fine wires.
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