Journal
GREEN CHEMISTRY
Volume 24, Issue 7, Pages 2946-2952Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d1gc04603a
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Funding
- China Scholarship Council
- University of Liverpool
- EPSRC [EP/R009694/1]
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A new protocol for the decarboxylative oxygenation of carboxylic acids using a non-heme manganese catalyst under blue light irradiation with O-2 as the sole oxidant is reported. The protocol allows readily available carboxylic acids to be converted into a wide variety of valuable compounds under mild reaction conditions.
Reported here is a new protocol for the decarboxylative oxygenation of carboxylic acids using a non-heme manganese catalyst under blue light irradiation with O-2 as the sole oxidant. Featuring mild reaction conditions, the protocol allows readily available carboxylic acids to be converted into a wide variety of valuable aldehydes, ketones and amides. Mechanistic studies indicate that the decarboxylation and oxygenation involves the formation of active Mn-oxygen species.
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