Journal
MATERIALS & DESIGN
Volume 107, Issue -, Pages 33-40Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.matdes.2016.06.017
Keywords
Carbon/carbon composites; Pyrocarbon; Heat treatment; Mechanical properties
Categories
Funding
- National Basic Research Program of China [2011CB605803]
- National Natural Science Foundation of China [51505503]
- Outstanding Graduate Project of Advanced Non-ferrous Metal Structural Materials and Manufacturing Collaborative Innovation Center
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Carbon fiber preforms were pre-heat treated at 2100 degrees C and then filled with smooth laminar (SL) pyrocarbon matrix by isothermal chemical vapor infiltration. The microstructure and flexural properties of carbon/carbon (C/C) composites after heat treatment from 1800 to 2500 degrees C were investigated. The microstructure investigation indicated that heat treatment did not affect the extinction angle, but resulted in distinct interfacial cracks and concentric cracks in the SL pyrocarbon. Three-point bending tests revealed that the flexural strength of the C/C composites decreased rapidly from 221 to 108 MPa after treated at 2100 degrees C. This can be explained that the multiple interfacial debonding and concentric cracks lead to poor stress transfer capabilities and high stress concentration. The flexural strength increased back to 126 MPa when the composites were heat treated under a higher temperature at 2500 degrees C. This phenomenon was attributed to cracks bridging in the debonding region and the thin high-textured layer at the fiber-matrix interface. (C) 2016 Elsevier Ltd. All rights reserved.
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