4.2 Article

An NMR Spectral Study of the Structure of 5,5,6-trihydroxy-6-methyldihydropyrimidine-2,4-(1H,3H)-dione in DMSO-d6

Journal

JOURNAL OF APPLIED SPECTROSCOPY
Volume 89, Issue 2, Pages 225-231

Publisher

SPRINGER
DOI: 10.1007/s10812-022-01347-z

Keywords

5; 5; 6-trihydroxy-6-methyldihydropyrimidine-2; 4(1H; 3H)-dione; NMR spectroscopy; dimethyl sulfoxide

Categories

Funding

  1. Russian Ministry of Science and Higher Education [102106231138681.4.1]

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The structure of 5,5,6-trihydroxy-6-methyldihydropyrimidine-2,4(1H,3H)-dione (2) was confirmed using C-13, H-1, and N-15 NMR spectroscopy. A new form (2a) was discovered, which has a similar structure to dione 2.
The structure of 5,5,6-trihydroxy-6-methyldihydropyrimidine-2,4(1H,3H)-dione (2) was proven using C-13, H-1, and N-15 NMR spectroscopy. A new form (2a) was detected and shown to have a structure similar to dione 2.

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