Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 3, Issue 6, Pages 749-752Publisher
CHINESE CHEMICAL SOC
DOI: 10.1039/c6qo00049e
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Funding
- 973 Program [2012CB725302]
- National Natural Science Foundation of China [21390400, 21520102003, 21272180, 21302148]
- Hubei Province Natural Science Foundation of China [2013CFA081]
- Research Fund for the Doctoral Program of Higher Education of China [20120141130002]
- Ministry of Science and Technology of China [2012YQ120060]
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A visible light mediated radical C-H phosphorization of benzothiazoles with O-2 as the sole oxidant was developed towards the synthesis of various 2-diarylphosphoryl benzothiazoles. The phosphonyl radical was identified by EPR experiments. In situ P-31 NMR experiments showed that Ph2P(O)H mainly converted into the desired product and the oxidative byproduct Ph2P(O)OH.
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