Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 3, Issue 11, Pages 1452-1456Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6qo00422a
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Funding
- NSFC [21232004, 21472071, 21602087]
- PAPD of Jiangsu Higher Education Institutions
- Outstanding Youth Fund of JSNU [YQ2015003]
- NSF of Jiangsu Province [BK20151163, BK 20160212]
- NSF of JSNU [14XLR005]
- Qing Lan
- NSF of Jiangsu Education Committee [15KJB150006]
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A new sulfonyl radical-triggered 6-endo-trig cyclization of unactivated 1,5-enynes under catalytic oxidation conditions for flexible synthesis of unprecedented unsymmetrical diaryl sulfones was established. This transformation could also proceed smoothly using 2-arylalkynyl-1,1'-biphenyls, delivering new sulfonylated phenanthrenes. The synthetic utility of these transformations results in subsequent C-S and C-C bond-forming reactions to effectively build up functional sulfones with potential significance.
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