Journal
NEW JOURNAL OF CHEMISTRY
Volume 46, Issue 30, Pages 14309-14313Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d2nj01197b
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Funding
- National Natural Science Foundation of China [21871087]
- Open Research Fund of Key Laboratory of Polar Materials and Devices, Ministry of Education
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A novel base-promoted strategy has been developed for the efficient preparation of medium-size-ring sulfonyl derivatives. This method involves alkynes insertion into the C-C sigma-bond of cyclic beta-keto sulfones, introducing sulfonyl groups into medium-size-ring compounds. The reaction demonstrates competitive features including broad substrate scope, transition-metal-free conditions, and atom economy.
A novel base-promoted and highly efficient strategy for the preparation of medium-size-ring sulfonyl derivatives has been developed. This method is realized by alkynes insertion into the C-C sigma-bond of cyclic beta-keto sulfones, introducing sulfonyl groups into medium-size-ring compounds. This reaction possesses competitive features such as broad substrate scope, transition-metal-free and atom economy.
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