4.7 Article

Synthesis of 1,2-oxazetidines with a free -NH group via photoredox catalysis

Journal

CHEMICAL COMMUNICATIONS
Volume 58, Issue 61, Pages 8508-8511

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/d2cc02892a

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A new photoredox approach has been reported for the one-step synthesis of oxazetidines with a free -NH group, using the combined use of alkyne, thiophenol, and azide. The synthesized oxazetidine with the -NH group was found to be stable enough for various late-stage transformations.
A photoredox approach enabling one-step synthesis of oxazetidines with a free -NH group via the combined use of alkyne, thiophenol, and azide has been reported. The synthesized oxazetidine with the free -NH group was stable enough for various late-stage transformations such as methylation, acetylation, tosylation, and ring-opening reaction to afford synthetically useful alpha-aminoketones.

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