Journal
JOURNAL OF SYNCHROTRON RADIATION
Volume 23, Issue -, Pages 1390-1394Publisher
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600577516014697
Keywords
soft X-ray; transmission mode; manganese oxide; in situ; operando; L-edge
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Funding
- Helmholtz Association [VH-NG-1140]
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A new cell for operando soft X-ray absorption spectroscopy in transmission mode is presented. Developed for investigations on solar water-splitting catalysts, the cell allows the study of solid films in direct contact with electrolyte solution while applying voltage and visible light. The design is optimized for fast sample exchange and the simultaneous measurement of fluorescence and transmission signal. The capability of the cell is presented on a manganese oxide (MnOx) film, where electronic structure changes are monitored during forward and backward potential changes. Detailed information about the varying contributions of several Mn oxidation states during this process was revealed.
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