Journal
CRYSTALS
Volume 6, Issue 11, Pages -Publisher
MDPI AG
DOI: 10.3390/cryst6110153
Keywords
mechanosynthesis; grinding; single-crystal structure; powder X-ray diffraction; maleic anhydride; tryptamine
Funding
- Televie Grant [F.R.S.-FNRS Televie 7.4.532.15.F]
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While mechanosynthesis of the target compound, 1-[2-(1H-indol-3-yl)-ethyl]-pyrrole-2,5dione, C-14 H-12 N-2 O-2, did not yield the desired product, it instead resulted in an open intermediate. On the other hand, synthesis starting from the activated maleic anhydride yielded the final maleimide compound. The outcome of the mechanosynthesis has been evaluated by powder X-ray diffraction, and structures of both the final product and open intermediate have been confirmed using single-crystal crystallography.
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