Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 9, Issue 21, Pages 5864-5871Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d2qo01224c
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Funding
- State Key Laboratory of Pulp and Paper Engineering [2020C02]
- National Natural Science Foundation of China [21971074]
- Natural Science Foundation of Guangdong Province [2019A1515010006, 2021A1515010159]
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An efficient synthesis of polysubstituted furans by Ag(i)-mediated annulation between 5-H-1,2,3-thiadiazoles and 1,3-dicarbonyl compounds is reported. The methodology is characterized by the availability of starting materials, good functional group tolerance, and the successful construction of heterocycle-substituted furans.
An efficient synthesis of polysubstituted furans by Ag(i)-mediated annulation between 5-H-1,2,3-thiadiazoles and 1,3-dicarbonyl compounds is reported. The methodology was characterized by availability of starting materials, good functional group tolerance, and the successful construction of heterocycle-substituted furans. The utilization of this method was evidenced by the gram-scale synthesis and further elaboration of the product. In addition, preliminary control experiments ruled out the formation of an alkynyl silver intermediate.
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