3.9 Article

New Method for the Synthesis of Phenylglyoxal Derivatives

Journal

DOKLADY CHEMISTRY
Volume 504, Issue 1, Pages 74-78

Publisher

MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0012500822600109

Keywords

phenylacrolein acetal; ozonolysis-reduction; carboxylic acid hydrazides; acylhydrazones

Funding

  1. Leader Project Competition, Ufa State Petroleum Technological University [15-2-22]
  2. Russian Academy of Sciences [1021062311392-9-1.4.1]

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The paper proposes a new one-pot ozonolytic synthesis of acylhydrazones from phenylacrolein acetals, using ozonolytic cleavage and treatment with various hydrazides.
The paper proposes a new one-pot ozonolytic synthesis of acylhydrazones from phenylacrolein acetals, which includes ozonolytic cleavage of the substrate in methanol and treatment of the intermediate peroxides with hydrazides of capric, nicotinic, isonicotinic, benzoic, and para-hydroxybenzoic acids taken in excess.

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