Journal
CHINESE JOURNAL OF ORGANIC CHEMISTRY
Volume 42, Issue 10, Pages 3398-3404Publisher
SCIENCE PRESS
DOI: 10.6023/cjoc202207009
Keywords
five-membered heterocycles; electrochemical synthesis; cross-dehydrogenative coupling reaction; dual roles; green chemistry
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Funding
- Natural Science Foundation of Hunan Province [2021JJ40429]
- Research Foundation of Education Bureau of Hunan Province [19B501]
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A practical method for the synthesis of various thiocyanated 5-membered aromatic heterocycles through electrochemical cross-coupling of heterocycles (pyrazoles, pyrroles, furans and thiophenes) with NH4SCN under chemical oxidant-and exogenous electrolyte-free conditions was developed.
A practical method for the synthesis of various thiocyanated 5-membered aromatic heterocycles through electrochemical cross-coupling of heterocycles (pyrazoles, pyrroles, furans and thiophenes) with NH4SCN under chemical oxidant-and exogenous electrolyte-free conditions was developed. NH4SCN played dual roles of a supporting electrolyte and a thiocyanated reagent, and thus simplify the reaction system.
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