4.4 Article

One-Step Hydrothermal Synthesis of CuO Micro-Crystals for Non-Enzymatic Glucose Sensors

Journal

SCIENCE OF ADVANCED MATERIALS
Volume 14, Issue 4, Pages 638-643

Publisher

AMER SCIENTIFIC PUBLISHERS
DOI: 10.1166/sam.2022.4241

Keywords

CuO Micro-Crystals; Hydrothermal; Non-Enzymatic Glucose Sensors

Funding

  1. National Natural Science Foundation of China [51802163]
  2. Training Program for Young Backbone Teachers of the Education Department of Henan Provincial [2020GGJS182]
  3. Colleges and Universities Key Scientific Research Project of Henan Province [21B140008]

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CuO micro-crystals were synthesized by a large-scale and environmentally friendly hydrothermal route. The CuO electrode exhibited excellent electrocatalytic performance for glucose oxidation, with fast response time, low detection limit, and applicable linear detection range. It also demonstrated good selectivity to glucose in the presence of interferences in human blood.
CuO micro-crystals have been synthesized by a one-step, large-scale and environment-friendly hydrothermal route. The crystalline structure, morphology, valence state and elemental composition of the CuO micro-crystals were analyzed using different technologies. Cyclic voltammetry and chronoamperometry were studied to probe the electrochemical glucose oxidation properties of the CuO electrode, revealing excellent electrocatalytic performance with fast response time, low detection limit and applicable linear detection range. In addition, it shows good selectivity to glucose when there are interferences coexisting in the human blood. All these results imply the potential application of the sample as electrode materials of non-enzymatic glucose sensors.

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