Journal
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
Volume 174, Issue -, Pages 106-119Publisher
JOURNAL MATER SCI TECHNOL
DOI: 10.1016/j.jmst.2023.05.051
Keywords
Stainless steel; Additive manufacturing; Rare earth; Precipitation; Tensile properties
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In this study, PH13-8Mo stainless steel parts doped with cerium were fabricated and compared with undoped parts. The doping of cerium improved the microstructure, phase constituents, and tensile properties of the stainless steel. The results showed that doping with cerium enhanced the mechanical stability of austenite, improved the sphericity of oxide inclusion, and increased the ultimate tensile strength and fracture elongation of the PH13-8Mo parts. The improved strength and ductility were attributed to the strengthening effects of nanoscale precipitation and grain refining, as well as the enhanced inclusion sphericity and coherency between the inclusion and matrix.
In this study, the PH13-8Mo stainless steel parts doped without and with cerium (Ce) were fabricated via laser powder bed fusion followed by post-heat treatment, and systematically compared in terms of microstructure, phase constituent, and tensile properties. The comparative results show that doping Ce-modified grains with the equiaxed morphology and finer size, increased the mechanical stability of austenite, and enhanced the sphericity of oxide inclusion in the resultant PH13-8Mo. Additionally, the coherency between the newly-formed CeAlO 3 inclusion and matrix was effectively im proved after doping Ce, as compared to the original aluminum oxide inclusion without doping Ce. The resultant PH13-8Mo parts doped with Ce yielded an ultimate tensile strength of 1446 & PLUSMN; 20 MPa with a fracture elongation of 16.0% & PLUSMN; 1.5%, for the first time meeting the AMS 5629E H10 0 0 standard for the PH13-8Mo made by additive manufacturing (AM). The enhanced strength results from the strengthening effects of nanoscale precipitation (inclusion) and grain refining. Meanwhile, the ductilizing mechanism can be attributed to the enhanced inclusion sphericity and ameliorative coherency between the inclusion and matrix, and improved misorientation angle of grain boundary owing to the modification by Ce, which efficiently reduced the stress concentration and enhanced cracking resistance during deformation. Therefore, doping rare earth elements presents a promising pathway to synergistically improve the strength and ductility of stainless steels by AM. & COPY; 2023 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.
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