4.6 Article

Synthesis, Optical, spectral and hardness properties of the novel Crystal: L-Arginium 5-Sulfosalicylate

Journal

MATERIALS LETTERS
Volume 353, Issue -, Pages -

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ELSEVIER
DOI: 10.1016/j.matlet.2023.135253

Keywords

Crystal Growth; Optical materials and Properties; XRD; UV-Vis; FTIR; Microhardness

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An organic crystal L-Arginium 5-Sulfosalicylate (A5SA) was synthesized using a slow evaporation method. The crystal was characterized by X-ray diffraction, UV absorbance, and fluorescence emission spectroscopy. It exhibited orange luminescence and a matched optical bandgap value according to Tauc's Plot.
An organic crystal L-Arginium 5-Sulfosalicylate (A5SA) was created by a slow evaporation method. The X-ray diffraction (XRD) analysis confirmed the novel cell parameters, a = 12.60 angstrom, b = 7.18 angstrom, c = 15.12 angstrom. The UV absorbance spectrum has a low cut-off wavelength at 243 nm. Optical bandgap of the crystal is 5.10 eV which matches with the Tauc's Plot. The fluorescence emission peak at 609 nm shows that the crystal emits orange luminescence. Fourier Transform Infrared (FTIR) and Raman (FT-Raman) analyses were used to analyse the spectrum investigations. The microhardness test confirmed that the grown crystal belongs to soft material category.

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