Journal
ORGANIC LETTERS
Volume 25, Issue 48, Pages 8570-8574Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.3c03355
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In this study, concise and divergent total syntheses of fusicoccane members brassicicenes A, R, and T were reported. The key feature of the synthesis is the rapid construction of the 5/8/5 tricyclic core via four steps, followed by concise oxidation state adjustment.
Here, we report concise and divergent total syntheses of fusicoccane members brassicicenes A, R, and T. The key feature of the synthesis is the rapid construction of the 5/8/5 tricyclic core via four steps: aldol reaction, Stork-Danheiser transposition, and ring-closing metathesis from known compounds followed by concise oxidation state adjustment.
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