Journal
CHEMICAL COMMUNICATIONS
Volume 59, Issue 45, Pages 6921-6924Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d3cc01766d
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Two amino-bridged bis(phenolate) neodymium complexes were synthesized and used as efficient initiators for the copolymerization of TMC and L-LA under mild conditions, resulting in the formation of random copolymers. NMR monitoring experiments confirmed the generation of a TMC/LA random copolymer through random copolymerization.
Random copolymerization of trimethylene carbonate (TMC) with l-lactide (LA) under mild conditions is a challenging task in polymer synthesis. Two amino-bridged bis(phenolate) neodymium complexes were synthesized and employed as efficient initiators for the copolymerization of TMC and l-LA under mild conditions to give random copolymers. NMR monitoring experiments of the chain microstructure versus polymerization time confirmed that a TMC/LA random copolymer was generated by a random copolymerization.
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