Journal
CHEMICAL COMMUNICATIONS
Volume 59, Issue 48, Pages 7391-7394Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d3cc02071a
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In this study, a catalytic method for the synthesis of primary amides was developed through the dehydrative condensation of carboxylic acids with aqueous ammonia using diboronic acid anhydride (DBAA) as the catalyst.
Although aqueous ammonia is an inexpensive and readily available safe source of ammonia, there have been no successful studies on direct catalytic dehydrative amidations of carboxylic acids with aqueous ammonia. In this study, we report a catalytic methodology for the synthesis of primary amides through diboronic acid anhydride (DBAA)-catalyzed dehydrative condensation of carboxylic acids with aqueous ammonia as the amine substrate.
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