Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 88, Issue 17, Pages 12738-12743Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.3c01429
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A straightforward synthetic approach for the construction of phenanthridin-6-(5H)-one skeletons is reported. Palladium catalysis is used to provide controlled access to a range of functionalized phenanthridin-6-(5H)-ones in yields of 59-88%. Plausible reaction pathways are proposed based on mechanistic experiments.
Herein, a straightforward synthetic approach for the construction of phenanthridin-6-(5H)-one skeletons is disclosed. The developed protocol relies on palladium catalysis, providing controlled access to a range of functionalized phenanthridin-6-(5H)-ones in 59-88% yields. Furthermore, plausible reaction pathways are proposed based on mechanistic experiments.
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