Journal
RSC ADVANCES
Volume 6, Issue 73, Pages 69595-69604Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ra11620e
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Funding
- Bu-Ali Sina University [BN093]
- Iran National Science Foundation (INSF) [BN093]
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Novel and recyclable thiourea dioxide-based magnetic nanoparticles with a sulfonic acid tag {Fe3O4@SiO2@(CH2)(3)-thiourea dioxide-SO3H/HCl} are described. The described catalyst was fully characterized using Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD) patterns, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), thermogravimetric analysis (TGA), atomic force microscopy (AFM) and ultraviolet-visible spectroscopy (UV/Vis). The reported novel magnetic nanocatalyst presents an excellent activity and catalytic performance for the synthesis of 1,1,3-tri(1H-indol-3-yl) alkane derivatives through one-pot three-component mixed Mannich-type and Friedel-Crafts reactions under solvent-free conditions at 60 degrees C.
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