Journal
CATALYSIS SCIENCE & TECHNOLOGY
Volume 6, Issue 21, Pages 7688-7692Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cy01400c
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- Ministry of Science and Technology, Taiwan
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We developed a technique mediated by visible light for the aerobic homocoupling of terminal alkynes to synthesize 1,3-conjugated diynes using a copper(I) chloride catalyst at room temperature. Compared with previously reported thermal processes, this photochemical method is simple, uses only mild reaction conditions, produces high yields and works well for substrates with electron-withdrawing groups without the need for bases/ligands, oxidants or palladium catalysts.
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