Journal
TETRAHEDRON LETTERS
Volume 57, Issue 22, Pages 2430-2433Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2016.04.083
Keywords
Halogenation; Alcohols; Halosilanes; Catalyst-free; Solvent-free
Categories
Funding
- Slovene Human Resources Development and Scholarship Fund [11011-9/2011]
- Slovenian Research Agency [P1-0134]
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A chemoselective method for the direct halogenation of different types of alcohols with halosilanes under catalyst- and solvent-free reaction conditions (SFRC) is reported. Various primary, secondary and tertiary benzyl alcohols and tertiary alkyl alcohols were directly transformed to the corresponding benzyl and alkyl halides, respectively, using chlorotrimethylsilane (TMSCI) and bromotrimethylsilane (TMSBr). (C) 2016 Elsevier Ltd. All rights reserved.
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