Journal
TETRAHEDRON
Volume 72, Issue 47, Pages 7594-7598Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2016.10.012
Keywords
Thiophosphates; Diphenylphosphine oxide; Sulfonyl chlorides; Direct synthesis
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A new method for the synthesis of thiophosphates by reductive coupling reaction of diphenylphosphine oxide and sulfonyl chlorides has been developed. The reaction is metal-free and needs no additives, affording various aryl and alkyl substituted thiophosphates in good to excellent yields under mild conditions. (C) 2016 Elsevier Ltd. All rights reserved.
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