Journal
TETRAHEDRON
Volume 72, Issue 49, Pages 8061-8065Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2016.10.042
Keywords
Malonate; Indolyl tetracarboxylates; Pd-catalyzed; Dehydrodimerization; C-H bond activation
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Funding
- NSF of China [21572072]
- Xiamen Southern Oceanographic Center [15PYY052SF01]
- Science and Technology Bureau of Xiamen City [3502Z20150054]
- Huaqiao University [ZQN-PY317]
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A novel dehydrodimerization of malonates with indoles has been developed, providing simple and rapid access to 3-indolyl tetramethyl 1,1,2,2-ethanetetracarboxylates. Pd(OAc)(2)-catalyzed 'one pot' C(sp(2))-C(sp(3)) and C(sp(3)) C(sp(3)) cross-dehydrogenative-couplings of malonates with a variety of 2-aryl indoles were involved. The titled compounds were obtained in high yields with good functional group tolerance. (C) 2016 Elsevier Ltd. All rights reserved.
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