Journal
TETRAHEDRON
Volume 72, Issue 49, Pages 8117-8122Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2016.10.066
Keywords
N-Boc-imines; Carbamoylsilanes; Amides; Addition; Synthetic methods
Categories
Funding
- Shanxi Province Foundation for Returness [0713]
- Natural Science Foundation of Shanxi Province [2012011046-9]
- Foundation of Shanxi Normal University, China [WL2015CXCY-YJ-21]
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N,N-Dimethylcarbamoyl(trimethyl)silane reacted with N-Boc-imines in anhydrous benzene under catalysts-free conditions to afford N-Boc-protected alpha-amino amides in good yields (72-89%). The electronic property and the steric hindrance of substituent on the N-Boc-imines affected the reaction. (C) 2016 Elsevier Ltd. All rights reserved.
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