Journal
SYNTHESIS-STUTTGART
Volume 49, Issue 1, Pages 115-120Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0036-1588318
Keywords
palladium(I) dimer; cross-coupling; Heck reaction; dinuclear catalysis; alkenes; catalyst recycling
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Funding
- RWTH Aachen University
- MIWF NRW
- Evonik Foundation
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The application of air- and moisture-stable dinuclear palladium(I) complex [Pd(mu-I)(Pt-Bu-3)](2) as an efficient catalyst for the Heck cross-coupling reaction of aryl iodides and bromides with acrylates and styrenes is described. The developed protocol is robust and operationally simple and shows a high functional-group tolerance. The employed palladium(I) dimer catalyst is highly robust under these nucleophilic as well as elevated-temperature conditions, allowing its recovery after reaction completion and recycling.
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