Journal
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY
Volume 152, Issue -, Pages 82-91Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.saa.2015.07.045
Keywords
Glass-ceramic; Molar ratio; Microstructure; Structure; Glass lattice
Categories
Funding
- NCBiR (Polish National Research and Development Committee) [N N508 477734, PBS1/B5/17/2012]
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This paper is focused on the effect of the molar ratio of SiO2/Al2O3 on the microstructure and structure of the internal aluminium silicon-oxide lattice of the glass ceramic materials from the SiO2-Al2O3-Na2O K2O-CaO system. In order to examine the real composition of the obtained samples, a chemical analysis was performed. Following the heat-treatment procedure, pseudowollastonite, anorthite and the vitreous phase were identified. In order to determine the microstructure, research using the scanning electron microscope (SEM) with EDS was done. For the inner structural study, X-ray diffraction (XRD), Raman spectroscopy as well as MIR and FIR spectroscopy were performed. (C) 2015 Elsevier B.V. All rights reserved.
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