Journal
SEPARATION AND PURIFICATION TECHNOLOGY
Volume 161, Issue -, Pages 165-171Publisher
ELSEVIER
DOI: 10.1016/j.seppur.2016.02.002
Keywords
Olive leaves; Polyphenols; DIC; Solvent extraction kinetics; Modeling
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Funding
- Ministere de l'Enseignement Superieur et de la Recherche Scientifique
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The aim of this investigation is to study the impact of the technology of instant controlled pressure drop: DIC on the kinetics extraction of olive leaf (Olea europaea L.) polyphenols. The conditions of extraction were: ethanol 95%, temperature: 55 degrees C and ratio r = 40 g g(-1) dry basis for 3 h. The extraction kinetics of total polyphenols content (TPC) of DIC-treated and untreated leaves were performed according to the method of Folin-Ciocalteau. The ultra-performance liquid chromatography (UPLC) was used to study the extraction kinetics of seven phenolic compounds of olive leaves: apigenin-7-glucoside, hydroxytyrosol, luteolin-7-glucoside, oleuropein, tyrosol, vanillic acid, and verbascoside. DIC-assisted solvent extraction allowed reducing the extraction time from 120 to 15 min while increasing the extracted yields. Phenomenological analysis of extraction kinetics was determined through the two-stage Coupled Washing/Diffusion CWD kinetic model. DIC texturing could, in favorable cases, increase the starting accessibility and systematically the internal effective diffusivity for phenolic compounds. (C) 2016 Elsevier B.V. All rights reserved.
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