Journal
RUSSIAN JOURNAL OF APPLIED CHEMISTRY
Volume 89, Issue 10, Pages 1619-1624Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S1070427216100094
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Results are presented obtained in tests of various homogeneous and heterogeneous catalysts in a synthesis of solketal (2,2-dimethyl-4-hydroxymethyl-1,3-dioxolane). It is shown that, all other conditions being the same, the highest catalytic activity is observed for sulfuric acid and beta zeolite. Data are presented on how the equilibrium constant of the reaction of glycerol ketalization depends on temperature. A technological scheme of the process for synthesis of solketal is suggested and its description is presented.
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