Journal
POLYMER ENGINEERING AND SCIENCE
Volume 56, Issue 5, Pages 583-589Publisher
WILEY
DOI: 10.1002/pen.24283
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Funding
- State Key Laboratory of Chemical Engineering [SKL-ChE-12A01]
- Postdoctor Science Foundation of China [2014M560802]
- Natural Science Foundation of Xi'an City [CXY1531WL31]
- NWU Scientific Research Foundation [PR13022, NG14028]
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TS-1 molecular sieves were synthesized and characterized by Fourier transform infrared spectroscopy, X-ray diffraction, scanning electron microscopy, thermogravimetric analysis, and UV-Vis spectroscopy. Results showed that the morphology, crystallinity, and purity of TS-1 were closely related to the Ti/Si ratio, crystallization time, crystallization temperature, and calcination time. The TS-1 particles were incorporated into polydimethylsiloxane to form mixed matrix membranes (MMMs), and these MMMs were first used to separate ethanol/water mixtures via pervaporation. The MMMs with 50 wt% TS-1 (Ti/Si ratio of 0.02) loading showed the highest separation factor of 14.1 for 5 wt% ethanol feed concentration at 50 degrees C. (C) 2016 Society of Plastics Engineers
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